Z A G R E B
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Original Scientific Paper
Preliminary Note
Review
Review Paper
Professional Paper
ARCHIVES 1996 - 2004
40
year issue
Metalurgija - Journal for Theory and Practice in Metellurgy
Metallurgy 64 (68) page
ISSN 1334-2576    UDC: 669+51+53+54(05)=862=20=30    METABK: 40 (4) 185 - 248 (2001)
Authors
Original Scientific Paper
E. Dudrová, M. Kabátová,
Ľ. Parilák, E. Košč
Microstructure and Properties of Fe-3Mn-Cx Sintered Steels
abstract, article page 187 - 194
L. Vehovar,
A. Vehovar, M. Tandler

The Corrosion Resistance of Austenitic Stainless Steel, Alloyed with Nitrogen
abstract, article page 195 - 200

Authors
Preliminary Note
J. Črnko, M. Kundak,
M. Gojić, Ž. Acs
Structure and Composition of the Scale on Steel Blooms Heated in a
Pusher-type Furnace
abstract, article page 201 - 205
J. Grum,
S. Božič, M. Zupančić
Influence of Quenching Process Parameters on Residual Stresses in Steels
abstract, article page 207 - 212
L. Fröhlich,
V. Mikloš
Leaching of As, Sb and Hg from Tetrahedrite Concentrate in the Na2S Medium at
Increased Temperatures
abstract, article page 213 - 218
E. Stroffek,
I. Lesso
Acoustic Method for Measurement of Young’s Modulus of Steel Wire Ropes
abstract, article page 219 - 221
Authors
Review Paper
V. Vítek
Study of Flow Pattern Solution Possibilities in the Furnace Zonal Models
abstract, article page 223 - 228
Authors
Professional Paper
I. Lesso

The Monitoring System of a Tunnel Furnace abstract, article page 229 - 231

J. Kizek,
Z. Zsigraiová
Combustion of Gaseous Fuels with high Content of Inert
abstract, article page 233 - 236
J. Kijac,
M. Pivovarči
Contribution to the Casting Powders Assimilation Power Study
abstract, article page 237 - 240
Authors
Review
I. Mamuzić
The Students of Faculty of Metallurgy University of Zagreb in 5th Technology
abstract, article page 241 - 243
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 Original Scientific Paper

E. Dudrová, M. Kabátová, Ľ. Parilák, E. Košč - Microstructure and Properties of Fe-3Mn-Cx Sintered Steels

    The influence of processing conditions (the influence of starting characteristics of powders, i. e. characteristics of iron powder as dominant and C and Mn as minor components, and processing conditions, such as pressing and sintering parameters) on mechanical properties and microstructure of Fe-3Mn-(0.26 - 0.9) %C are analyzed in the paper. At suitable processing conditions the tensile strength higher than 650 MPa, hardness higher than 200 HV 30, impact energy up to 17 J cm-2, and 3-point bend strength higher than 1000 MPa were achieved. From the viewpoint of iron powder and Mn-alloying component used, the sponge iron NC 100.24 and electrolytical manganese seem to be advantageous when compared with iron powders SC 100.26 and ASC 100.29 and ferromanganese powders. The highest strength properties correspond to carbon content of 0.6 %. In sintering processes, the cooling rate of 40 °C/min is more advantageous than 10 °C/min.

L. Vehovar, A. Vehovar, M. Tandler - The Corrosion Resistance of Austenitic Stainless Steel, Alloyed with Nitrogen

     The results of corrosion investigations have shown that, even in a very aggressive medium, the austenitic nitrogen-enriched stainless steel NTR50, which was solution heat treated at 1150 °C/ quenched - i.e. steel with interstitially dissolved nitrogen in the austenitic base, passivizes directly at a low anodic current density. This is the not case for the comparative AISI 316L stainless steel, although the pitting potentials of both materials are similar. However, significant differences exist between the repassivation capability of nitrogen-enriched steel and that of the comparative AISI 316L steel, which can be attributed to the important role of the nitrogen. Investigations of the passive film confirmed that nitrogen, in the form of N3- and NH4+ ions, acts as an inhibitor of the corrosion process. This means that the time for the initiation of corrosion pits, which are usually the source of stress corrosion cracking, is extended. Due to rapid changes in the character of the electrolyte in the corrosion crack and the repulsing action of the N3- ions towards the aggressive chloride ions, the growth of the crack is either prevented or greatly retarded.

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Preliminary Note
J. Črnko, M. Kundak, M. Gojić, Ž. Acs - Structure and Composition of the Scale on Steel Blooms Heated in a Pusher-type Furnace

    Samples of a scale formed on steel blooms heated in a pusher-type furnace are investigated by optic microscopic examination and by X-ray diffraction method. The results of investigation by means of optic microscopy have shown that the scale consisted of a thinner outer layer and thicker inner layer. Thickness of the layers of the scale increases by the increase of the heating time of steel blooms. The inner layer of the scale is porous while the outer layer consisted of grain structure. By X-ray diffraction method it was found that both layers of the scale consists of FeO (wüstite), a-Fe2O3 (hematite) and Fe3O4 (magnetite). Possible reasons for the scale dropping off on the botton of the heating zone of the pusher-type furnace during heating of steel materials at temperatures of hot working were discussed.


J. Grum, S. Božič, M. Zupančić -
Influence of Quenching Process Parameters on Residual Stresses in Steels

     Increasing demands of users regarding ensurance of the specified mechanical properties and working order of machine parts and products require a search of relations between the composition and microstructure and certain knowledge of residual stresses present based on good knowledge of the quenching process. The paper presents results regarding numerous residual stresses measurements on heat-treatment 42CrMo4 steel specimens with different masses. To measure the residual stresses, the relaxation method was used, involving gradual mechanical removal of the hardened layer in which the deformation of the specimen was measured by resistance strain gauges.

L. Fröhlich, V. Mikloš - Leaching of As, Sb and Hg from Tetrahedrite Concentrate in the Na2S Medium at Increased Temperatures

    The present article contains knowledge about an alternative method of hydrometallurgical processing of the Slovak tetrahedrite concentrate from the area of Rudňany. The stated concentrate is characterized by its high content of Hg, order of units of mass %. It also contains other dominant accompanying elements - As and Sb. Our experimental study monitored the efficiency of leaching the stated accompanying elements into solutions with various concentrations of Na2S, without and with the addition of 30 g/l NaOH, at increased temperatures. A rotary autoclave without the possibility of intensive mixing was used, which had an impact on the results obtained, mainly in the area of kinetic study. Leaching within a temperature range between 120 °C and 220 °C under various conditions was performed, in a six series of experiments. The results obtained show the suitability of using the autoclave process for the extraction of As, Sb and Hg from the tetrahedrite concentrate into a basic solution of Na2S.

E. Stroffek, I. Lesso - Acoustic Method for Measurement of Young’s Modulus of Steel Wire Ropes


     The classical methods for estimation of Young’s modulus of steel wire ropes are time consuming. One of the additional disadvantages of these methods is that they could not be applied in situ but only in laboratories. We have designed a new acoustical method and as the results show it seems to be promising and usable in plant. In this contribution we compare the results of Young’s modulus measurement with the new method for different wire and charge conditions.

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Review Paper

V. Vítek - Study of Flow Pattern Solution Possibilities in the Furnace Zonal Models

    The present paper deals with the conditions estimation for the flow pattern solution possibilities inside the furnace as dependant on the inner space division in the volume zones. Provided solutions with the application of the free and finite turbulent stream model show that in principle it is possible to solve rather complex problems for the need of the zone models without the necessity to solve the sets of the partial differential equations for the case of the viscous flowing media. The methodology of the solution process and the results are presented for the flow pattern estimation in the chamber furnace equipped with two burners and for the flow patter inside the tunnel kiln out of the burners zone.

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Professional Paper
I. Lesso - The Monitoring System of a Tunnel Furnace

     Various types of refractory materials are in the tunnel furnace fired in the temperature interval 1450 - 1700 °C. The tunnel furnace is approximately 160 m long and consists of 53 modules with three heating zones: warming, firing and colding, operating in upstream regime. In the paper the use of IBM PC compatible computers for the design of small on-line real-time systems is presented.

J. Kizek, Z. Zsigraiová - Combustion of Gaseous Fuels with high Content of Inert

    In the paper authors deal with experimental investigation of an inert gas influence on combustion parameters of gaseous fuels such as flame stability and outlet velocity. The aim is to supplement knowledge of combustion process of gaseous fuel with high content of inert compounds.

J. Kijac, M. Pivovarči -
Contribution to the Casting Powders Assimilation Power Study

    T he main characteristics of the casting powders for the continuous casting - their chemical composition, melting temperature, dynamic viscosity and specific consumption. Decisive factors of casting powders effect CC course. Effect of the casting powders properties on the cast products surface quality. Same field experiment results obtained with variety of casting powders application based on the domestic production (MOLDCAST). Evaluation of assimilation ability. Change of chemical composition of the CC casting powder in course of the casting. Ability of casting powders to absorb the alumina inclusions. Change of the physical and chemical parameters of the formed slag in course of casting. Analysis of the obtained information.

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ARCHIVES 1996. - 2000. (under construction): author(s) - name of the article - abstract